[Rockhounds] DIY XRD?

Hans Durstling siniconb at gmail.com
Thu Oct 23 09:30:42 PDT 2008


Kitchen-table affordable Xrays should be no problem at all. Back in
the days when people still tinkered and I could buy nitric acid at the
corner drug store I remember reading in one of the scientific hobby
publications that certain early radio tubes were a generous source of
incidental Xrays and could be modified to make them much more so. Or
given even rudimentary glass blowing ability and access to a good
vacuum pump you should be able to make your own tube. Then all you'd
need is a high voltage DC power supply which likely could be scavenged
from a television, a computer or some other domestic device, thus
leaving the bulk of the budget for lead and concrete; you wouldn't
want to skimp on that.

Cheers,
Hans Durstling
Moncton, Canada
typing two handed again, broken arm mending





On 10/23/08, J Bryan Kramer <codeburner at gmail.com> wrote:
> It has been known for a year or two that lightning not only produces X-Rays
>  it produces Gamma.
>
>  <http://cat.inist.fr/?aModele=afficheN&cpsidt=15675313>
>
>  <http://news.ufl.edu/2003/01/30/lightxray/>
>
>  <http://news.nationalgeographic.com/news/2007/10/071011-lightning-rays.html>
>
>
>  BK
>
>
>  On Thu, Oct 23, 2008 at 09:55, <Pmodreski at aol.com> wrote:
>
>  > Ah, yes, now, let's not throw too much cold water on Kreigh's cool  idea.
>  > Who knows, "in theory" it might work, but in practice... yeah, the  amount
>  > of
>  > X-rays produced are probably very miniscule, and although in theory  one
>  > might
>  > filter out just one wavelength of X-rays, in practice what one is  starting
>  > with is probably too spread over a range of X-ray wavelengths, to be
>  >  useful.
>  > And the X-rays are probably emitted in all directions, not focused
>  > geometrically at all, so by the time one collimated just the ones traveling
>  > in a
>  > particular direction toward the sample, one would again lose 99% of the
>  > tiny  amount
>  > that had been produced...  There was also the caveat in the story,  that
>  > the
>  > X-rays were only detectable when the experiment was done in a vacuum
>  >  chamber.
>  >
>  > I wonder, if a miniscule amount of X-rays are produced in any electrical
>  > discharge, where high-voltage electrons are hitting something; as in a
>  > lightning
>  > bolt, or even, in a static electricity discharge when you shuffle across
>  > the
>  > rug  and touch your finger to something metal?  Seems like that and the
>  > Scotch
>  >  Tape, are just different versions of the same thing.  That would be even
>  > the simpler way to generate the X-rays for Kreigh's homemade
>  > mini-diffractometer!
>  >
>  > Cheers, and keep at it, Kreigh,
>  > Pete
>  >
>  >
>  > In a message dated 10/22/2008 7:49:23 P.M. Mountain Daylight Time,
>  > Kreigh at tomaszewski.net writes:
>  >
>  > Bryan,
>  >
>  > The Bragg Equation requires the wavelength. Coherent  x-rays from an
>  > incoherent source are fairly easy to produce using a small  aperture
>  > monochromator. That problem was solved about a hundred years  ago.
>  >
>  > I agree that the real problem is the energy. There has to be  enough at
>  > some wavelength to produce a detectable beam out of the filtered
>  > source. I assume there is enough since they were able to x-ray a
>  > finger, but it might require a slower scan than a commercial unit; it
>  > is easy to make x-ray detection cumulative.
>  >
>  > How long will a roll of  tape last? How many times can it be reused? I
>  > would be really happy to be  able to get an analysis for the cost of a
>  > roll of  tape.
>  >
>  > Kreigh
>  >
>  >
>  >
>  >
>  > On Wednesday, Oct 22, 2008, at 20:58  America/Detroit, J Bryan Kramer
>  > wrote:
>  >
>  > > Doesn't x-ray  energy/wavelength make a difference for x-ray
>  > > diffraction? I
>  > >  read that scotch tape article and it didn't sound like you could
>  > >  control
>  > > much beyond being able to produce some sort of x-rays in  bursts.
>  > >
>  > > BK
>  > >
>  > > On Wed, Oct 22, 2008 at 20:44,  Kreigh Tomaszewski
>  > >  <Kreigh at tomaszewski.net>wrote:
>  > >
>  > >> I've often wished I  could move a lab into my basement and do x-ray
>  > >>  analysis
>  > >> of minerals, but cost makes it just a  dream.
>  > >>
>  > >> Now it has been discovered that unrolling  scotch take in a vacuum
>  > >> produces
>  > >>  x-rays.
>  > >>
>  > >>  http://news.yahoo.com/s/ap/20081022/ap_on_sc/sci_scotch_tape_surprise
>  > >>
>  > >>  Using a roll of tape, a small motor to unwind it, and a vacuum pump,
>  > >> to
>  > >> produce a source of x-rays turns the dream into a  possible do it
>  > >> yourself
>  > >>  project.
>  > >>
>  > >> The database for comparison against known  minerals is available at
>  > >> places
>  > >> such as  http://rruff.geo.arizona.edu/AMS/amcsd.php. The rest of the
>  > >>  details are relatively trivial once you have a source of  x-rays.
>  > >>
>  > >>  http://productsearch.machinedesign.com/mdproducts/x_ray_diffraction
>  > >>
>  > >>  Anybody interested in a science project?
>  > >>
>  > >>  Kreigh
>  > >>
>  > >>
>  > >> --
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>  North Florida, USA
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